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Modified microwave method for the synthesis of visible light-responsive TiO2/MWCNTs nanocatalysts

Firas K Mohamad Alosfur14*, Mohammad Hafizuddin Haji Jumali1*, Shahidan Radiman1, Noor J Ridha14, Mohd Ambar Yarmo2 and Akrajas Ali Umar3

Author affiliations

1 School of Applied Physics, Faculty Science and Technology, Universiti Kebangsaan Malaysia, Bangi, Selangor 43600, Malaysia

2 School of Chemical Sciences and Food Technology, Faculty of Science and Technology, Universiti Kebangsaan Malaysia (UKM), Bangi, Selangor 43600, Malaysia

3 Institute of Microengineering and Nanoelectronic (IMEN), Universiti Kebangsaan Malaysia, Bangi, Selangor 43600, Malaysia

4 Physics Department, Science College, Baghdad University, Baghdad, Iraq

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Citation and License

Nanoscale Research Letters 2013, 8:346  doi:10.1186/1556-276X-8-346

Published: 6 August 2013

Abstract

Recently, TiO2/multi-walled carbon nanotube (MWCNT) hybrid nanocatalysts have been a subject of high interest due to their excellent structures, large surface areas and peculiar optical properties, which enhance their photocatalytic performance. In this work, a modified microwave technique was used to rapidly synthesise a TiO2/MWCNT nanocatalyst with a large surface area. X-ray powder diffraction, field-emission scanning electron microscopy, transmission electron microscopy and Brunauer-Emmett-Teller measurements were used to characterise the structure, morphology and the surface area of the sample. The photocatalytic activity of the hybrid nanocatalysts was evaluated through a comparison of the degradation of methylene blue dye under irradiation with ultraviolet and visible light. The results showed that the TiO2/MWCNT hybrid nanocatalysts degraded 34.9% of the methylene blue (MB) under irradiation with ultraviolet light, whereas 96.3% of the MB was degraded under irradiation with visible light.

Keywords:
Microwave; TiO2/MWCNTs; Hybrid nanocatalysts; Photocatalytic